第1章 逸出气体分析简介 Introduction to Evolved Gas Analysis(1)
第2章 热重-质谱联用技术TGA-MS(6)
2.1质谱的原理 Principles of MS(6)
2.2TGA-MS 测量系统 The TGA-MS System(8)
2.3测量模式 Measurement Modes(9)
2.4结果解释 Interpretation of Results(11)
2.5典型的碎片化模式 Typical Fragmentation Patterns(15)
2.6结果表述 Presentation of Results(16)
第3章 热重-红外光谱联用技术TGA-FTIR (17)
3.1FTIR的原理 Principles of FTIR(17)
3.2TGA-FTIR系统 The TGA-FTIR System(21)
3.3曲线表示 Presentation of Results(22)
3.4解析方法 Interpretation Procedure(24)
3.5光谱的解析 Interpretation of Spectra(26)
3.6特征吸收频率 Characteristic Absorption Frequencies(27)
3.7结果表述 Presentation of Results(29)
第4章 热重分析-气相色谱/质谱联用技术TGA-GC/MS (30)
4.1GC的原理 Principles of GC(30)
4.2TGA-GC/MS系统 The TGA-GC/MS System(35)
4.3测量可行性 Measurement Possibilities(36)
4.4测量结果 Results(39)
第5章 热重分析-微型气相色谱/质谱联用技术TGA-Micro GC/MS (41)
5.1微型气相色谱仪的原理 Principles of Micro GC(41)
5.2TGA-Micro GC和TGA-Micro GC/MS系统
TGA-Micro GC and TGA-Micro GC/MS Systems(44)
5.3实验结果 Results(45)
第6章 应用简介 Introduction to the Applications (46)
第7章应用介绍 Applications List (49)
7.1通过TGA-MS、TGA-FTIR和TGA-MicroGC研究一水合草酸钙的分解机理
Decomposition of Calcium Oxalate Monohydrate (Tutorial) by TGA-MS,
TGA-FTIR and TGA-Micro GC(55)
7.2通过TGA-MS和TGA-FTIR研究五水合硫酸铜的分解机理
Decomposition of Copper Sulfate Pentahydrate (Tutorial)
by TGA-MS and TGA-FTIR(57)
7.3实验条件对MS灵敏度的影响分析
Influence of Experimental Conditions on MS Sensitivity(59)
7.4通过TGA-MS和TGA-GC/MS多次进样法研究乙酰水杨酸的分解
Decomposition of Acetylsalicylic Acid by TGA-MS and TGA-GC/MS Multi-injection(65)
7.5通过TGA-FTIR研究BHET的热降解
Thermal Degradation of BHET by TGA-FTIR(67)
7.6通过TGA-FTIR研究工业月桂醇的分解
Decomposition of Technical Lauryl Alcohol by TGA-FTIR(70)
7.7通过TGA-MS检测药物中的残留溶剂
Detection of Residual Solvents in a Pharmaceutical Substance by TGA-MS(72)
7.8通过TGA-MS研究填充有机物的沸石的解吸附
Desorption of a Zeolite Filled with Organic Matter by TGA-MS(73)
7.9通过TGA-MS研究PVC粉末的热裂解
Pyrolysis of PVC Powder by TGA-MS(76)
7.10通过TGA-FTIR研究氟化电缆线
Investigation of Fluorinated Cable Wires by TGA-FTIR(78)
7.11通过TGA-MS检测橡胶样品中的水杨酸甲酯
Detection of Methyl Salicylate in a Rubber Sample by TGA-MS(80)
7.12通过TGA-FTIR研究有机硅聚合物的降解
Degradation of a Silicone Polymer by TGA-FTIR(81)
7.13通过TGA-MS和TGA-FTIR研究氨基树脂的固化和分解
Curing and Decomposition of an Amino Resin by TGA-MS and TGA-FTIR(83)
7.14通过TGA-FTIR和DSC研究热转变和分解以鉴别BR和NR橡胶
Identification of BR and NR Rubbers. Study of Thermal Transitions and Decomposition
by TGA-FTIR and DSC(85)
7.15通过TMA-MS研究印刷电路板的分层
Delamination of Printed Circuit Boards by TMA-MS(88)
7.16通过TMA-MS研究用于封装发泡剂的聚合物的膨胀和分解
Expansion and Decomposition of a Polymer Used To Encapsulate a Blowing Agent
by TMA-MS(89)
7.17通过TGA-MS测定离子液体中的水分含量
Determination of the Water Content of an Ionic Liquid by TGA-MS(91)
7.18通过TGA-FTIR研究热裂解并阐明阻燃机理
From the Investigation of Pyrolysis to the Elucidation of Fire Retardancy Mechanisms
by TGA-FTIR(93)
7.19通过TGA-MS和DSC研究高熔点陶瓷
High Melting Ceramics by TGA-MS and DSC(97)
7.20通过TGA-MS和显微DSC研究唑来膦酸水合物的热行为
Thermal Behavior of Zoledronic Acid Hydrate by TGA-MS and DSC-Microscopy(100)
7.21通过TGA-MS定量分析钴粉中的氧化钴
Quantification of Cobalt Oxide in a Coated Cobalt Powder by TGA-MS(103)
7.22通过TGA-GC/MS和TGA-Micro GC/MS研究聚酰胺66的分解产物
Investigation of Evolved Decomposition Products of Polyamide66
by TGA-GC/MS and TGA-Micro GC/MS(104)
7.23通过TGA-GC/MS、DSC和DMA鉴定多组分热塑性树脂
Identification of Multi-Component Thermoplastics by TGA-GC/MS, DSC and DMA(107)
7.24通过TGA-GC/MS、DSC、DMA和ATR研究橡胶的变形原因
Deformulation of a Rubber by TGA-GC/MS, DSC, DMA and ATR(113)
7.25通过TGA-GC/MS-FTIR测定聚丙烯材料有无磷酸铵阻燃剂的性质
Polypropylene with and without Ammonium Phosphate Flame Retardant
by TGA-GC/MS-FTIR(120)
7.26通过TGA-GC/MS对EPDM橡胶进行热氧化研究
Thermal Oxidation of EPDM Rubber by TGA-GC/MS(125)
7.27通过TGA-MS和TGA-GC/MS定量分析涂料中的二甲基甲酰胺（DMF）
Quantification of Dimethylformamide in Coatings by TGA-MS and TGA-GC/MS(129)
7.28TGA-GC/MS定量测定天然橡胶中低含量的丁苯橡胶
Quantification of a Low Content of Styrene-Butadiene Rubber in Natural Rubber
by TGA-GC/MS(134)
7.29通过TGA-Micro GC/MS技术分析酚醛树脂的分解产物
Evolved Decomposition Products of a Phenol-Formaldehyde Resin
by TGA-Micro GC/MS(137)
7.30通过TGA-Micro GC/MS技术定量分析焦炭样品中的二氧化碳
Quantification of Carbon Dioxide in a Coke Sample by TGA-Micro GC/MS(140)
7.31TGA-Micro GC/MS、TMA和DSC用于钛酸钡的合成和表征
Synthesis and Characterization of Barium Titanate by TGA-Micro GC/MS, TMA and DSC(142)
7.32用TGA-Micro GC/MS和Karl Fischer滴定仪测定热塑性塑料中的水含量
Determination of Water Content in a Thermoplastic by TGA-Micro GC/MS
and Karl Fischer titrator(147)
7.33通过TGA-GC/MS和TGA-Micro GC/MS研究生物质样品
Study of a Biomass Sample by TGA-GC/MS and TGA-Micro GC/MS(151)
7.34通过 TGA-GC/MS和TGA-Micro GC/MS分析由褐煤释放出的气体
Gases Evolved from Lignite by TGA-GC/MS and TGA-Micro GC/MS(157)
参考书目 Literature(164)
缩写和首字母缩写词 Abbreviations and Acronyms(165)
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